Synthesis, structure and spectroscopic characterization of 1,2-bis-(2,4,6-trimethylbenzylideneamino)ethanedichloropalladium(II)
Makaleler > Tam Makale · 2006
Yazarlar: Cengiz Arici, DinÇer ülkü, İsmail Özdemir, Serpil Demir, Bekir Çetinkaya
Journal of Coordination Chemistry, Uluslararası, Wos, 2006, cilt 59, ss 797-802
DOI: 10.1080/00958970500404609
Özet
The structure of 1,2-bis(2,4,6-trimethylbenzylideneamino)ethanedichloropalladium(II) was determined by X-ray diffraction methods. The structure derived from NMR and IR spectra and elemental analysis is consistent with it. The complex is orthorhombic, space group Pcab, with a = 14.8662(12), b = 15.0861(13), c = 20.6255(14) Å, V = 4625.7(6) Å3 and Z = 8. In the lattice, there exists a weak C–H ··· Cl hydrogen bond.